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Chemical Reactor - Laboratory Report, Study Guides, Projects, Research of Chemical Processes

Chemical Reactor with sodium hydroxide and ethyl acetate. PFR reactor and CSTR reactor.

Typology: Study Guides, Projects, Research

2017/2018

Uploaded on 12/30/2018

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CHEMICAL ENGINEERING PROGRAM
CHME 401 – Chemical Engineering Laboratory II
Experiment # 4
Chemical Reactors
Group B
Submitted by:
Leader Mehdi Raza Nanji 2175529
Experimenter Khawaja Hamza 2127801
Data Taker Busra Tepe 2018596
Submitted to: Aykut Argonul
Date of Experiment: 2018-12-13
Date of Submission: 2018-12-27
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CHEMICAL ENGINEERING PROGRAM

CHME 401 – Chemical Engineering Laboratory II Experiment # 4 Chemical Reactors

Group B Submitted by: Leader Mehdi Raza Nanji 2175529 Experimenter Khawaja Hamza 2127801 Data Taker Busra Tepe 2018596

Submitted to: Aykut Argonul Date of Experiment: 2018-12- Date of Submission: 2018-12-

Declaration of Independent Work

We, the undersigned, hereby declare that

  • The presented report is our authentic work
  • We have not received any help, document or data from any other party
  • (^) We have not falsified or fabricated the presented experimental data
  • Neither did we make use of any other groups’ reports and calculations, nor will we provide our reports and calculations to any other group
  • We have not committed plagiarism and therefore we have given reference to all the sources we have used as a reference

Date: 2018-12- Mehdi Raza Nanji _______________ Khawaja Hamza _______________ Busra Tepe _______________

Table of Contents

Declaration of Independent Work.................................................................................. i

Abstract.........................................................................................................................ii

Table of Contents......................................................................................................... iii

List of Figures............................................................................................................... v

List of Tables

  • Introduction................................................................................................................... List of Tables................................................................................................................ vi
    • Objective...................................................................................................................
    • Background...............................................................................................................
    • Theory.......................................................................................................................
      • Continuous Stirred Tank Reactor (CSTR).............................................................
      • Plug Flow Reactor (PFR)......................................................................................
      • Rate of Reaction...................................................................................................
      • Order of Reaction..................................................................................................
      • Reaction Stoichiometry.........................................................................................
  • Experimental Method....................................................................................................
    • Experimental Setup..................................................................................................
    • Experimental Procedure...........................................................................................
  • Results..........................................................................................................................
    • Experimental Data....................................................................................................
      • Calibration curve...................................................................................................
      • CSTR – 100 % flow...............................................................................................
      • CSTR – 75 % flow.................................................................................................
      • PFR – 100 % flow.................................................................................................
      • PFR – 75 % flow...................................................................................................
      • PFR – 50 % flow.................................................................................................
    • Calculated Data......................................................................................................
      • Calibration curve.................................................................................................
      • CSTR..................................................................................................................
      • PFR.....................................................................................................................
  • Discussion..................................................................................................................
  • Conclusion..................................................................................................................
  • References.................................................................................................................
  • Nomenclature.............................................................................................................
  • Appendix.....................................................................................................................
    • Calculations............................................................................................................
  • Table 1 – Calibration standard solutions with conversions...........................................
  • Table 2 – Calibration data.............................................................................................
  • Table 3 – CSTR experimental data at 100 % flow........................................................
  • Table 4 – CSTR experimental data at 75 % flow..........................................................
  • Table 5 – PFR experimental data at 100 % flow...........................................................
  • Table 6 – PFR experimental data at 75 % flow.............................................................
  • Table 7 – PFR experimental data at 50 % flow...........................................................
  • Table 8 – CSTR results..............................................................................................
  • Table 9 – PFR results.................................................................................................
  • Table 10 – Set up data [1]...........................................................................................
  • Table 11 – Flow rates.................................................................................................
  • Table 12 – Conversion data........................................................................................
  • Table 13 – CSTR calculations....................................................................................
  • Table 14 – PFR calculations.......................................................................................

Introduction

Objective

This experiment studies two different reactors, a tubular reactor and a continuously stirred tank reactor, in the production of sodium acetate from sodium hydroxide and ethyl acetate. The experiments objective is to analyze the performance of each reactor and to study the effect of feed flow rates [1].

Background

For any reactor, the general mole balance for any component A, can be expressed as below in Equation 1 Equation SEQ Equation * ARABIC 1

Group BMETU NCC – CHME 401 2018-1Page 13 of 20